Synthesis and Characterization of Alumina Zirconia Composite Material Doped with Silica

Manas Ranjan Majhi, S. Viswakarma, N. S. Meheta., K. Sauravh, S. Singhand

Abstract


Present research work deals with synthesis of alumina zirconia silica Composite material by mixed powder composed of varying weight percentage of alumina and silica with fixed 30% weight composition of zirconia. The characteristics such as bulk density, apparent porosity, linear shrinkage and weight loss behaviour, XRD, bending strength and micro structures of different samples were analysed comparatively with gradual increment of silica content from 0 to 4wt% into base composition. After sintering at 1200°C, samples shows significant change in its physical and microstructural properties such as densification and reduction in apparent porosity, XRD pattern reveal zirconium aluminium oxide phase with conversion of monoclinic zirconia to tetragonal phase and bending strength ware also improved apparently. Micro structure analysis of sintered composite gives relative grain sizes and phases present in different samples which shows improved bonding between the matrixes with silica addition.


Keywords


Alumina Zirconia, Silica, XRD pattern

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References


Modern Refractory Practice. Harbison-Walker Refractories Company, Cleveland. 1961. 452 pages.

Norton FH. Refractories. Mc-Graw Hill Book Company, 1968.

Szutkowska M. Fracture Resistance Behaviour of Alumina-Zirconia Composites. Journal of Materials Processing Technology 2004; 153-154: 868-74.

Casellas D, Rafols I, Llanes L, et al. Fracture Toughness of Zirconia-Alumina Composites. International Journal of Refractory Metals and Hard Materials 1999; 17(1-3): 11-20.

Zhiquiang C, Feng QIN. Synthesis of Zirconia-Alumina Ultrafines Composites and their Sintering Behaviour. China Refractories 1997; 6(1).

Fukai S. Alumina-Zirconia Material Properties and Application to Refractories. Taikabutsu, 2002.

Asokan T. Microstructural features of fusion cast Al2O3-ZrO2-SiO2 refractories. Journal of Materials

Science Letters 1994; 13(5): 343-5.

Garcia CM. Applied Physics and Mechanical Engineering, Lulea University, 2008.

Marchi J, Bressiani AHA, Bressiani JC. Densification studies of silicon carbide based ceramics with yttria, silica and alumina as additives. Materials Research 2001; 4(4): 231-6.

Martinelli AE, Paulo DSA, Nascimento RM, et al. Dilatometric behaviour and microstructure of sintered Fe-NbC and Fe-TaC composites. Journal of Material Science 2007; 42(1): 314-9.


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